Structural characterization of SnO nanoparticles synthesized by the hydrothermal and microwave routes (2020)
- Authors:
- USP affiliated authors: BATISTA, FABIO RODOLFO MIGUEL - EEL ; BACANI, REBECA - EEL ; TRIBONI, EDUARDO REZENDE - EEL ; DIAS, JULIANA DA SILVA - IEA
- Unidades: EEL; IEA
- DOI: 10.1038/s41598-020-66043-4
- Subjects: SINTERIZAÇÃO; NANOPARTÍCULAS
- Agências de fomento:
- Language: Inglês
- Abstract: SnO particles were synthesized by an alkali-assisted hydrothermal and microwave methods. The aqueous-based reactions were carried out at pH ~ 8, under inert atmosphere (Ar). The reactions were taken under different times, and a full XRD structural analysis was made to evaluate the conversion from the Sn6O4(OH)4 intermediate to SnO particles. Williamson-Hall analysis showed that the size and strain of the SnO particles were time and route treatment dependent. Microwave heating yielded a single tetragonal SnO phase after 1 h of thermal treatment, and TEM images revealed spherical-shaped SnO nanoparticles with an average size of 9(1) nm. While by the hydrothermal treatment single SnO phase was obtained only after 4 hours, yielding non-uniform and elongated particles with sub-micrometric size. A dissolution-recrystallization process was taken into account as the mechanism for SnO particles formation, in which hydroxylated complexes, Sn2(OH)6−2, then condense to form the oxide. The time-shorting reaction provided by the microwave-assisted synthesis may be attributed to better heat distribution.
- Imprenta:
- Source:
- Título: Scientific Reports
- ISSN: 2045-2322
- Volume/Número/Paginação/Ano: v. 10, p. 1-11, 2020
- Status:
- Artigo publicado em periódico de acesso aberto (Gold Open Access)
- Versão do Documento:
- Versão publicada (Published version)
- Acessar versão aberta:
-
ABNT
DIAS, Juliana S. et al. Structural characterization of SnO nanoparticles synthesized by the hydrothermal and microwave routes. Scientific Reports, v. 10, p. 1-11, 2020Tradução . . Disponível em: https://doi.org/10.1038/s41598-020-66043-4. Acesso em: 07 maio 2026. -
APA
Dias, J. S., Batista, F. R. M., Bacani, R., & Triboni, E. R. (2020). Structural characterization of SnO nanoparticles synthesized by the hydrothermal and microwave routes. Scientific Reports, 10, 1-11. doi:10.1038/s41598-020-66043-4 -
NLM
Dias JS, Batista FRM, Bacani R, Triboni ER. Structural characterization of SnO nanoparticles synthesized by the hydrothermal and microwave routes [Internet]. Scientific Reports. 2020 ; 10 1-11.[citado 2026 maio 07 ] Available from: https://doi.org/10.1038/s41598-020-66043-4 -
Vancouver
Dias JS, Batista FRM, Bacani R, Triboni ER. Structural characterization of SnO nanoparticles synthesized by the hydrothermal and microwave routes [Internet]. Scientific Reports. 2020 ; 10 1-11.[citado 2026 maio 07 ] Available from: https://doi.org/10.1038/s41598-020-66043-4 - Optical and structural characterization of ZnO nanoparticles with different morphologies for photocatalytic applications,
- Synthesis and characterization of tin oxide nanoparticles
- Self-assembled Mg(OH) gels driving to MgO nanoribbons
- A simplified and general approach to distillation with parallel streams: the cases of para- and metastillation
- A simplified and general approach to distillation with parallel streams: the cases of para- and metastillation
- A new unified model to simulate columns with multiple phase divisions and their impact on energy savings
- Properties of microalgae oil from the species Chlorella protothecoides and its ethylic biodiesel.
- Columns with multiple phase divisions: simulation and application in crude oil distillation
- A simplified and general approach to absorption and stripping with parallel streams
- Influence of the liquid or vapor split ratios in meta- or para-stillation columns
Informações sobre a disponibilidade de versões do artigo em acesso aberto coletadas automaticamente via oaDOI API (Unpaywall).
Por se tratar de integração com serviço externo, podem existir diferentes versões do trabalho (como preprints ou postprints), que podem diferir da versão publicada.
How to cite
A citação é gerada automaticamente e pode não estar totalmente de acordo com as normas
